3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟-1-癸硫醇合成路线 （共 16 条）
34143-74-33,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟-1-癸硫醇+
→
反应条件
potassium carbonate in acetonitrile T=50°C;
参考文献
Christensen, Caspar; Clausen, Rasmus P.; Begtrup, Mikael; Kristensen, Jesper L.
Tetrahedron Letters, 2004 , vol. 45, # 43 p. 7991 - 7993
34143-74-33,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟-1-癸硫醇
→
反应条件
potassium carbonate in acetonitrile T=50°C;
参考文献
Christensen, Caspar; Clausen, Rasmus P.; Begtrup, Mikael; Kristensen, Jesper L.
Tetrahedron Letters, 2004 , vol. 45, # 43 p. 7991 - 7993
34143-74-33,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟-1-癸硫醇+
→
反应条件
potassium carbonate in ethanol
T=75°C; 6 h;
参考文献
Pees; Cahuzac; Sindt; Ameduri; Paul; Boutevin; Mieloszynski
Journal of Fluorine Chemistry, 2001 , vol. 108, # 2 p. 133 - 142
34143-74-33,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟-1-癸硫醇+
→
反应条件
2,2'-azo-bisisobutyronitrile
T=80°C; 4 h; Title compound not separated from byproducts;
参考文献
Pees; Cahuzac; Sindt; Ameduri; Paul; Boutevin; Mieloszynski
Journal of Fluorine Chemistry, 2001 , vol. 108, # 2 p. 133 - 142
34143-74-33,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟-1-癸硫醇
→
反应条件
hydrogenchloride; iodine; dimethyl sulfoxide
Oxidation; 1.16667 h; Heating;
参考文献
Brace, Neal O.
Journal of Fluorine Chemistry, 2000 , vol. 105, # 1 p. 11 - 23
34143-74-33,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-十七氟-1-癸硫醇
→
反应条件
3-chloro-benzenecarboperoxoic acid in ethyl acetate
T=-28°C; Oxidation; 12 h;
参考文献
Brace, Neal O.
Journal of Fluorine Chemistry, 2000 , vol. 102, # 1-2 p. 21 - 41
