1: benzo[b]thiophene With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 0.5 h; Inert atmosphere; 2: benzyl bromide in tetrahydrofuran; pentane T=-78 - 20°C; Inert atmosphere;
参考文献
Urban, Slawomir; Beiring, Bernhard; Ortega, Nuria; Paul, Daniel; Glorius, Frank
Journal of the American Chemical Society, 2012 , vol. 134, # 37 p. 15241 - 15244
K10-ZnCl2 in nitromethane T=20°C; 0.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Clark, Peter D.; Kirk, Andrew; Mesher, Shaun T.; Yee, James G.K.
Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 96, # 1-4 p. 441 - 444
1: 84 percent / K10-ZnCl2 / 300 °C / 0.03 Torr 2: K10-ZnCl2 / nitromethane / 0.5 h / 20 °C View Scheme
参考文献
Clark, Peter D.; Kirk, Andrew; Mesher, Shaun T.; Yee, James G.K.
Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 96, # 1-4 p. 441 - 444
