反应条件
1: 1.) NaH / 1.) benzene, RT, 30 min, 2.) toluene, benzene, RT, overnight
2: 97 percent / p-toluenesulfonic acid / CH2Cl2 / 2 h / Ambient temperature
3: 68 percent / diethyl ether / 2 h
4: 90 percent / p-TsOH / methanol / 2 h / Ambient temperature
5: 87 percent / pyridine / CH2Cl2 / 12 h / Ambient temperature
6: 90 percent / n-Bu4NF / tetrahydrofuran / 1.5 h / Ambient temperature
7: 96 percent / 1N aq.KOH / methanol / 0.17 h / Ambient temperature
View Scheme
参考文献
Nagatsuki, Fumi; Sasaki, Shigeki; Maeda, Minoru
Journal of Fluorine Chemistry, 1992 , vol. 56, # 3 p. 373 - 383
