2-氯-5-硝基二苯甲酮合成路线 (共 12 条)
反应条件
aluminium trichloride 1 h; Heating;
参考文献
Hayashi, Ikuo; Ogihara, Keizo; Shimizu, Kiyoshi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2432 - 2437
反应条件
aluminium chloride in benzene
参考文献
SANOFI
Patent: US4980349 A1, 1990 ;
反应条件
1: 93.1 percent / phosphorus pentachloride / benzene / 3 h / Heating 2: 85.4 percent / aluminium chloride / 1 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 8 p. 2432 - 2437
反应条件
phosphorus pentachloride man fuegt AlCl3 hinzu und zersetzt mit Eis;
参考文献
Chemische Berichte, , vol. 39, p. 300
反应条件
potassium fluoride 12 h; Heating;
参考文献
Frigola; Colombo; Mas; Pares
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 2 p. 399 - 407
反应条件
ethanol; hydroxylamine hydrochloride T=140 - 150°C; im Rohr;
参考文献
Meisenheimer; Zimmermann; v. Kummer
Justus Liebigs Annalen der Chemie, 1926 , vol. 446, p. 225
反应条件
potassium hydroxide in water T=150 - 160°C; 5 h;
参考文献
Hayashi, Ikuo; Ogihara, Keizo; Shimizu, Kiyoshi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2432 - 2437
反应条件
potassium hydroxide in water; ethylene glycol
参考文献
Bristol-Myers Company
Patent: US4056540 A1, 1977 ;
US 4056540 A
反应条件
ammonia T=160°C; im geschlossenen Rohr;
参考文献
Ullmann; Mallet
Chemische Berichte, 1898 , vol. 31, p. 1695
参考文献
Ullmann; Mallet
Chemische Berichte, 1898 , vol. 31, p. 1695