2-氯-4'-硝基苯乙酮合成路线 （共 22 条）
反应条件
1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione; toluene-4-sulfonic acid in methanol T=30 - 35°C; 8 h;
参考文献
Xu, Zijin; Zhang, Deyan; Zou, Xinzhuo
Synthetic Communications, 2006 , vol. 36, # 2 p. 255 - 258
反应条件
N-chloro-succinimide; toluene-4-sulfonic acid in acetonitrile 1 h; Reflux;
参考文献
Zhu, Yan-Ping; Cai, Qun; Gao, Qing-He; Jia, Feng-Cheng; Liu, Mei-Cai; Gao, Meng; Wu, An-Xin
Tetrahedron, 2013 , vol. 69, # 31 p. 6392 - 6398
反应条件
S4N4*SbCl5 in toluene 3 h; Heating;
参考文献
Kim, Kil-Joong; Kim, Kyongtae
Tetrahedron Letters, 1997 , vol. 38, # 24 p. 4227 - 4230
反应条件
[2,2']bipyridinyl; copper(l) chloride in 1,2-dichloro-ethane 3 h; Heating;
参考文献
Ram, Ram N.; Manoj
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5633 - 5635
反应条件
1: With methanol; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) 261 h; Heating; 2: With hydrogenchloride; water in tetrahydrofuran T=65°C; 20 h;
参考文献
Krane Thvedt, Thor Hakon; Fuglseth, Erik; Sundby, Eirik; Hoff, Bard Helge
Tetrahedron, 2009 , vol. 65, # 46 p. 9550 - 9556
反应条件
chlorine dioxide in tetrachloromethane T=52 - 54°C; 2 h;
参考文献
Kwiecien, Halina; Jalowiczor, Jozef
Polish Journal of Chemistry, 1986 , vol. 60, # 7-12 p. 811 - 824
反应条件
Oxone®; ammonium chloride T=20°C; 24 h;
参考文献
Zhou, Zhong-Shi; Li, Li; He, Xue-Han
Journal of Chemical Research, 2013 , vol. 37, # 10 p. 633 - 635
反应条件
in tetrachloromethane T=130°C; other temperatures; Rate constantThermodynamic data;
参考文献
McDonald, Richard N.; Cousins, Raymond C.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 2976 - 2984
反应条件
hydrogenchloride in 1,4-dioxane; water Rate constant;
参考文献
Wagenaar,A. et al.
Journal of Organic Chemistry, 1974 , vol. 39, # 3 p. 411 - 414
参考文献
Miyahara,Y.
Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 1147 - 1151
