2-(1-环己烯基)乙胺合成路线 （共 34 条）
反应条件
ammonia; hydrogen; chromium; cobalt; iron; nickel in methanol T=100°C; P=60004.8 Torr;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 12 p. 1487 - 1493
反应条件
lithium aluminium tetrahydride in di-isopropyl ether 1.) 5 deg C, 1 h, 2.) RT, 2 h;
参考文献
Passarotti; Valenti; Grianti
Bollettino Chimico Farmaceutico, 1993 , vol. 132, # 11 p. 472 - 474
反应条件
1: With iodine in methanol T=20°C; 7 h; 2: With zinc in methanol T=20°C; 0.5 h;
参考文献
Vatele, Jean-Michel
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9127 - 9130
反应条件
triethylsilane; triethylamine; palladium diacetate in dichloromethane T=23°C; Hydrogenolysis; 12 h;
参考文献
Synthesis, , # SPEC. ISS. p. 1399 - 1400
反应条件
1: NaBH4 / methanol; H2O / 1 h / Ambient temperature 2: acetic anhydride / 6 h / Heating 3: 89.5 percent / lithium aluminum hydride / diisopropyl ether / 1.) 5 deg C, 1 h, 2.) RT, 2 h View Scheme
参考文献
Bollettino Chimico Farmaceutico, , vol. 132, # 11 p. 472 - 474
反应条件
1: acetic anhydride / 6 h / Heating 2: 89.5 percent / lithium aluminum hydride / diisopropyl ether / 1.) 5 deg C, 1 h, 2.) RT, 2 h View Scheme
参考文献
Bollettino Chimico Farmaceutico, , vol. 132, # 11 p. 472 - 474
反应条件
2: LiAlH4 View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 32, # 3 p. 950 - 956
反应条件
Raney Co; ammonia; hydrogen in methanol T=100°C; P=60004.8 Torr; Product distribution; Further Variations:Reagents;
参考文献
Journal of Catalysis, , vol. 234, # 1 p. 161 - 171
反应条件
lithium aluminium tetrahydride
参考文献
Helvetica Chimica Acta, , vol. 33, p. 1437,1447
反应条件
1: With hydrogen; palladium 10 on activated carbon in methanol; acetic acid T=20°C; 76 h; 2: With hydrogenchloride in dichloromethane
参考文献
Diaz, Caroline Jean; Haffner, Curt Dale; Speake, Jason Daniel; Zhang, Cunyu; Mills, Wendy Yoon; Spearing, Paul Kenneth; Cowan, David John; Green, Gary Martin
Patent: US2010/222345 A1, 2010 ;
Location in patent: Page/Page column 107 ;
