13(S)--过氧羟基-9,11-十八碳二烯酸合成路线 (共 5 条)
反应条件
1: lipase 2: 49 percent / DCC, dimethylaminopyridine / CHCl3 3: 65 percent / CH3COOH / tetrahydrofuran; H2O 4: 44 percent / NaBH4 / methanol / 0.25 h / 0 °C View Scheme
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 56, # 2.3.4 p. 540
反应条件
allene oxide synthase in phosphate buffer T=0°C; pH=7.0; 0.00555556 h;
参考文献
Medvedeva; Latypov; Balandina; Mukhtarova; Grechkin
Russian Journal of Bioorganic Chemistry, 2005 , vol. 31, # 6 p. 595 - 596
Title/Abstract Full Text View citing articles Show Details
Medvedeva, Natalia V.; Mukhtarova, Lucia S.; Mukhitova, Faina K.; Balandina, Alsu A.; Latypov, Shamil K.; Grechkin, Alexander N.
Chemistry and Physics of Lipids, 2007 , vol. 148, # 2 p. 91 - 96
反应条件
sulfuric acid
1.) H2O, room temp., 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Gardner, H. W.; Weisleder, D.; Nelson, E.C
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 508 - 515
反应条件
sulfuric acid
1.) H2O, room temp., 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Gardner, H. W.; Weisleder, D.; Nelson, E.C
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 508 - 515
反应条件
sulfuric acid
1.) H2O, room temp., 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Gardner, H. W.; Weisleder, D.; Nelson, E.C
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 508 - 515