in methanol byproducts: NH3, CH3OH; all manipulations in Ar atm.; soln. of CsOMe in MeOH added to soln. of NH4 compd. in MeOH; concd., filtered or pumped to dryness at 25°C;
参考文献
Haiges, Ralf; Christe, Karl O.
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 8 p. 1717 - 1718
acetic acid in methanol to a soln. of Cs2CO3 in MeOH is added dropwise acetic acid, stirred for1 h at ambient temp.; MeOH is removed under reduced pressure;
in neat (no solvent) thermolysis in the absence of O2 at 420°C;
参考文献
Santalova, N. A.; Seisenbaeva, G. A.; Dunaeva, K. M.; Spitsyn, V. I.
Doklady Chemistry (English Translation), 1988 , vol. 300, p. 182 - 184
Doklady Akademii Nauk SSSR, 1988 , vol. 300, p. 1143 - 1146
