反应条件
1: 1) 9-BBN, 2) NaOH, H2O2 / 1) THF, 20 deg C, 2 h; 2) water, 20 deg C, 3 h. 2: 95 percent / pyridine / 1) -5 deg C, 0.5 h; 2) 0 deg C, 6 h. 3: 82 percent / hexamethylphosphoric acid triamide; tetrahydrofuran / 10 h / 0 - 5 °C 4: 95 percent / hydrogen, quinoline / Lindlar catalyst / hexane / 3 h 5: 1) 9-BBN, 2) NaOH, H2O2 / 1) THF; 2) water. View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 20, # 4 p. 486 - 489
Khimiya Prirodnykh Soedinenii, , vol. 20, # 4 p. 514 - 518
