1-(甲氧基甲基)-4-甲基苯合成路线 （共 44 条）
反应条件
N-ethyl-N,N-diisopropylamine; C26H24BrOPPd; triphenylphosphine T=28 - 47°C; P=2587.76 Torr; Conversion of starting material;
参考文献
HERIOT-WATT UNIVERSITY
Patent: WO2006/10885 A1, 2006 ;
Location in patent: Page/Page column 26; 31 ;
反应条件
1: With dicarbonyl(pentamethylcyclopentadienyl)(4-methoxyphenyl)iron in dichloromethane 4 h; Inert atmosphereIrradiationSchlenk technique; 2: With sodium hydroxide in methanol; water Schlenk techniqueInert atmosphere;
参考文献
Argouarch, Gilles; Grelaud, Guillaume; Roisnel, Thierry; Humphrey, Mark G.; Paul, Frederic
Tetrahedron Letters, 2012 , vol. 53, # 37 p. 5015 - 5018
反应条件
in methanol; diethyl ether 15 h; Heating;
参考文献
Bernasconi, Claude F.; Sun, Weitao
Journal of the American Chemical Society, 2002 , vol. 124, # 10 p. 2299 - 2304
反应条件
sodium hydride in diethylene glycol dimethyl ether; Petroleum ether T=55 - 90°C; 2.5 h;
参考文献
Strazzolini, Paolo; Runcio, Antonio
European Journal of Organic Chemistry, 2003 , # 3 p. 526 - 536
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=80°C; 20 h;
参考文献
Kosugi, Masanori; Sumiya, Takashi; Ogata, Toshimi; Sano, Hiroshi; Migita, Toshihiko
Chemistry Letters, 1984 , p. 1225 - 1226
反应条件
iron (III) perchlorate T=20°C; 1 h; neat (no solvent);
参考文献
Behbahani, Farahnaz K.; Heravi, Majid M.; Oskooie, Hossien A.
Monatshefte fur Chemie, 2009 , vol. 140, # 2 p. 181 - 184
反应条件
ytterbium(III) triflate T=145°C; 3 h; microwave irradiation;
参考文献
Handlon, Anthony L.; Guo, Yu
Synlett, 2005 , # 1 art. no. S08204ST, p. 111 - 114
反应条件
iodine T=20°C; 0.533333 h;
参考文献
Kumar; Anjaneyulu; Joyasawal, Sipak; Pawan Chakravarthy; Naveen Kumar; Yadav
Journal of the Indian Chemical Society, 2007 , vol. 84, # 2 p. 189 - 192
反应条件
in tetrahydrofuran; methanol 0.25 h;
参考文献
ASTRAZENECA AB
Patent: WO2007/8140 A1, 2007 ;
Location in patent: Page/Page column 191 ;
WO 2007/008140 A1
反应条件
iodine T=20°C; 0.666667 h;
参考文献
Kumar; Anjaneyulu; Joyasawal, Sipak; Pawan Chakravarthy; Naveen Kumar; Yadav
Journal of the Indian Chemical Society, 2007 , vol. 84, # 2 p. 189 - 192
