1-(二甲氧基甲基)-4-甲基苯合成路线 (共 28 条)
反应条件
sodium methylate; lithium perchlorate; TDBPA in dichloromethane indirect electrochemical oxidation;
参考文献
Brinkhaus, Karl-Heinz Grosse; Steckhan, Eberhard; Degner, Dieter
Tetrahedron, 1986 , vol. 42, # 2 p. 553 - 560
反应条件
lithium in tetrahydrofuran T=20°C; 24 h;
参考文献
Azzena, Ugo; Denurra, Teresa; Melloni, Giovanni; Piroddi, Anna Maria
Journal of Organic Chemistry, 1990 , vol. 55, # 20 p. 5532 - 5535
反应条件
3,3-dimethyldioxirane in acetone T=25°C; Kinetics;
参考文献
Baumstark; Kovac, Franci; Vasquez, Pedro C.
Heterocyclic Communications, 2002 , vol. 8, # 1 p. 9 - 12
反应条件
1: 90 percent / HClO4-SiO2 / H2O; methanol / 0.17 h / 25 - 30 °C 2: 95 percent / HClO4-SiO2 / 0.17 h / 25 - 30 °C View Scheme
参考文献
Kumar, Raj; Kumar, Dinesh; Chakraborti, Asit K.
Synthesis, 2007 , # 2 p. 299 - 303
参考文献
Surmont, Riccardo; Verniest, Guido; De Klmpe, Norbert
Organic Letters, 2009 , vol. 11, # 13 p. 2920 - 2923
反应条件
triethylsilane; acetyl-bromide; stannous bromide in dichloromethane 3 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Tsukamoto, Kazuhisa; Ichimura, Yuichi; Koga, Gen
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1410 - 1412
反应条件
hafnium tetrachloride in acetonitrile T=20°C; Strecker Aminoacid Synthesis; 0.5 h; Inert atmosphere;
参考文献
Zhang, Xue-Lin; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2013 , vol. 37, # 11 p. 690 - 693
反应条件
sodium tetrafluoroborate; sulfuric acid 1.) anodic oxidation, AcOH, 2.) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nishiguchi, Ikuzo; Hirashima, Tsuneaki
Journal of Organic Chemistry, 1985 , vol. 50, # 4 p. 539 - 541
反应条件
sodium tetrafluoroborate; sulfuric acid 1.) anodic oxidation, AcOH, MeOH, 2.) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nishiguchi, Ikuzo; Hirashima, Tsuneaki
Journal of Organic Chemistry, 1985 , vol. 50, # 4 p. 539 - 541
反应条件
sodium tetrafluoroborate; sulfuric acid 1.) anodic oxidation, AcOH, 2.) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nishiguchi, Ikuzo; Hirashima, Tsuneaki
Journal of Organic Chemistry, 1985 , vol. 50, # 4 p. 539 - 541