3-硝基苯甲醛二甲基乙缩醛合成路线 （共 18 条）
反应条件
Decaborane in methanol T=20°C; 2 h;
参考文献
Kumar, Raj; Kumar, Dinesh; Chakraborti, Asit K.
Synthesis, 2007 , # 2 p. 299 - 303
反应条件
Br(1-)*C19H14Br3O3PS*Na(1+) T=20°C;
参考文献
Huo, Congde; Chan, Tak Hang
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1933 - 1938
反应条件
1: HNO3; H2SO4 / CH2Cl2 / 6 h / 20 °C 2: conc. HCl / 144 h / 25 °C View Scheme
参考文献
Icke et al.
Organic Syntheses, 1955 , vol. Coll. Vol. III, p. 644
反应条件
1: O2 / H2O / Irradiation 2: trimethyl orthoformate / Heating View Scheme
参考文献
Wan, Peter; Muralidharan, S.; McAuley, Iain; Babbage, Christopher A.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1775 - 1783
反应条件
1: CH3CN, Na2SO3 / H2O 2: trimethyl orthoformate / Heating View Scheme
参考文献
Wan, Peter; Muralidharan, S.; McAuley, Iain; Babbage, Christopher A.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1775 - 1783
反应条件
pyridine-2-carboxylic acid; iron sulphate heptahydrate; dihydrogen peroxide T=20 - 60°C; 12 h; Schlenk techniqueMolecular sieve;
参考文献
Ray, Ritwika; Chowdhury, Abhishek Dutta; Lahiri, Goutam Kumar
ChemCatChem, 2013 , vol. 5, # 8 p. 2158 - 2161
反应条件
hydrogenchloride; methanol
参考文献
Cocker; Harris; Loach
Journal of the Chemical Society, 1938 , p. 751
参考文献
Claisen
Chemische Berichte, 1898 , vol. 31, p. 1020
反应条件
methanol; sodium hydroxide; water
参考文献
Schmitz
Chemische Berichte, 1958 , vol. 91, p. 410,412
反应条件
(i) HNO3, H2SO4, (ii) /BRN= 3592982/, MeOH; Multistep reaction;
参考文献
Kuffner,F. et al.
Monatshefte fuer Chemie, 1960 , vol. 91, p. 1152 - 1161
