1,2-二甲氧基-4-二硝基苯合成路线 （共 69 条）
反应条件
1: 130 - 135 °C
2: phosphoric acid; arsenic acid / 100 °C
3: SnCl2; aqueous HCl
View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, vol. 77, p. 4819
参考文献
Parijs
Recueil des Travaux Chimiques des Pays-Bas, 1930 , vol. 49, p. 33,41
反应条件
1: boron tribromide / dichloromethane / -78 °C
2: potassium carbonate / N,N-dimethyl-formamide
View Scheme
参考文献
Marks, Patrick; Cohen, Sage; Levine, Mindy
Journal of Polymer Science, Part A: Polymer Chemistry, 2013 , vol. 51, # 19 p. 4150 - 4155
反应条件
1: H2 / Raney nickel / tetrahydrofuran / 60 °C
2: triethylamine / tetrahydrofuran
3: potassium carbonate / dimethylformamide / 0.75 h / Heating
View Scheme
参考文献
Descours, Denis; Festal, Didier
Synthesis, 1983 , # 12 p. 1033 - 1036
反应条件
1: H2 / Raney nickel / tetrahydrofuran / 60 °C
2: triethylamine / tetrahydrofuran / 1 h
View Scheme
参考文献
Descours, Denis; Festal, Didier
Synthesis, 1983 , # 12 p. 1033 - 1036
反应条件
1: aqueous HBr
2: ethanol; iron-powder; aqueous HCl / anschliessend Umsetzung mit dem Dinatrium-Salz der 1,2-Dihydroxy-aethan-1,2-disulfonsaeure
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参考文献
Ehrlich; Bogert
Journal of Organic Chemistry, 1947 , vol. 12, p. 522,529
反应条件
1: H2 / 10percent Pd/C / methanol / Ambient temperature
2: methanol / 21 h / Ambient temperature
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参考文献
Alcalde, E; Dinares, I; Frigola, J
European Journal of Medicinal Chemistry, 1991 , vol. 26, # 6 p. 633 - 642
反应条件
1: 130 - 135 °C
2: phosphoric acid; arsenic acid / 100 °C
View Scheme
参考文献
Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1542
反应条件
1: palladium/charcoal; ethanol / Hydrogenation
2: acetic acid; aqueous HCl
View Scheme
参考文献
Weinberger; Day
Journal of Organic Chemistry, 1959 , vol. 24, p. 1451,1452, 1453
