2,3,7-三氯二苯并-对-二恶英合成路线 （共 5 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; potassium hydroxide; potassium carbonate 2.) 180 deg C; Multistep reaction;
参考文献
Luebke, Markus; Whitcombe, Michael J.; Vulfson, Evgeny N.
Journal of the American Chemical Society, 1998 , vol. 120, # 51 p. 13342 - 13348
反应条件
in methanol; water Irradiation(60)Co-γ-radiolysis; isomerisation, conversion into trichlorodibenzodioxin and decomposition; doses dependence 0.2-10.0 Mrad; Product distribution;
参考文献
Qin, Zhaohai
Chemosphere, 1996 , vol. 33, # 1 p. 91 - 97
反应条件
18-crown-6 ether; chlorine; acetic acid Yield given. Title compound not separated from byproducts;
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Chernov, S. A.
Doklady Chemistry, 1992 , vol. 327, # 1-3 p. 245 - 247
Doklady Akademii Nauk SSSR, 1992 , vol. 327, # 1 p. 92 - 95
反应条件
oxygen T=500°C; var. reactor medium; Rate constant;
参考文献
Samsonov, D. P.; Rakhmanova, T. V.; Peryunina, R. I.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 1.2 p. 182 - 187,149 - 154
反应条件
1: trifluoroacetic anhydride, ammonium nitrate / nitromethane
2: hydrazine hydrate / Raney nickel / tetrahydrofuran; ethanol / Heating
View Scheme
参考文献
Luebke, Markus; Whitcombe, Michael J.; Vulfson, Evgeny N.
Journal of the American Chemical Society, 1998 , vol. 120, # 51 p. 13342 - 13348
