3,5-二叔丁基邻苯醌合成路线 (共 229 条)
反应条件
3-chloro-benzenecarboperoxoic acid in tetrahydrofuran
参考文献
Funabiki,T.; Mizoguchi,A.; Sugimoto,T.
Journal of the American Chemical Society, 1986 , vol. 108, p. 2921
反应条件
potassium peroxomonosulphate in 1,4-dioxane; methanol; water
T=10°C; phosphate buffer pH 7;
参考文献
Ando, Wataru; Miyazaki, Hajime; Akasaka, Takeshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 9 p. 518 - 519
反应条件
potassium peroxomonosulphate in 1,4-dioxane; water
T=10°C; phosphate buffer pH 7;
参考文献
Ando, Wataru; Miyazaki, Hajime; Akasaka, Takeshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 9 p. 518 - 519
反应条件
disodium hydrogenphosphate; potassium dihydrogenphosphate; dihydrogen peroxide
1.) aq.MeOH, 7 d; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Speier, Gabor; Tyeklar, Zoltan
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1176 - 1179
反应条件
disodium hydrogenphosphate; potassium dihydrogenphosphate; dihydrogen peroxide in methanol; water
Product distribution;
参考文献
Speier, Gabor; Tyeklar, Zoltan
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1176 - 1179
反应条件
disodium hydrogenphosphate; potassium dihydrogenphosphate; dihydrogen peroxide in methanol; water
ΔH(excit.), ΔS(excit.); KineticsThermodynamic dataMechanism;
参考文献
Speier, Gabor; Tyeklar, Zoltan
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1176 - 1179
反应条件
1: With ammonium hydroxide in methanol
T=20°C; 0.166667 h;
2: With sodium tetrahydroborate
参考文献
Lodyato, Vladimir I.; Yurkova, Irina L.; Sorokin, Viktor L.; Shadyro, Oleg I.; Dolgopalets, Vladimir I.; Kisel, Mikhail A.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 6 p. 1179 - 1182
反应条件
in ethanol; water
T=50°C; 5 h;
参考文献
Vinsova, Jarmila; Horak, Vaclav; Buchta, Vladimir; Kaustova, Jarmila
Molecules, 2005 , vol. 10, # 3 p. 760 - 770
反应条件
in ethanol; water
T=50°C; 5 h;
参考文献
Vinsova, Jarmila; Horak, Vaclav; Buchta, Vladimir; Kaustova, Jarmila
Molecules, 2005 , vol. 10, # 3 p. 760 - 770
反应条件
in ethanol; water
T=50°C; 5 h;
参考文献
Vinsova, Jarmila; Horak, Vaclav; Buchta, Vladimir; Kaustova, Jarmila
Molecules, 2005 , vol. 10, # 3 p. 760 - 770