3,5-二叔丁基邻苯醌合成路线 （共 229 条）
反应条件
in benzene inert atmosphere; heating (ampoule fused, 100°C, 48 h); further products;
参考文献
Journal of Organometallic Chemistry, , vol. 443, # 1 p. 43 - 49
反应条件
1: 75 percent / 1,2-ethylenediamine / H2O; propan-2-ol / 2 h / Heating
2: 80 percent / 1.5 h / 80 °C
View Scheme
参考文献
Jimenez-Perez, Victor M.; Camacho-Camacho, Carlos; Gueizado-Rodriguez, Marisol; Noeth, Heinrich; Contreras, Rosalinda
Journal of Organometallic Chemistry, 2000 , vol. 614-615, p. 283 - 293
反应条件
in benzene
inert atmosphere; heating (ampoule fused, 80°C, 48 h); further products;
参考文献
Riviere-Baudet, Monique; Morere, Alain; Khallaayoun, Abdelhay
Journal of Organometallic Chemistry, 1993 , vol. 443, # 1 p. 43 - 49
反应条件
in benzene-d6
inert atmosphere (Ar or N2); 120°C, 12 h; not isolated; identified by (1)H-NMR and MS;
参考文献
Riviere-Baudet, M.; Riviere, P.; Khallaayoun, A.; Satge, J.; Rauzy, K.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 77 - 94
反应条件
in benzene
inert atmosphere; heating (ampoule fused, 100°C, 48 h); further products;
参考文献
Riviere-Baudet, Monique; Morere, Alain; Khallaayoun, Abdelhay
Journal of Organometallic Chemistry, 1993 , vol. 443, # 1 p. 43 - 49
反应条件
in benzene-d6
inert atmosphere (Ar or N2); 20°C, 12 h; not isolated; identified by (1)H-NMR and MS;
参考文献
Riviere-Baudet, M.; Riviere, P.; Khallaayoun, A.; Satge, J.; Rauzy, K.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 77 - 94
反应条件
in benzene
Kinetics; byproducts: Me2NNMe2, EtNMe2; inert atmosphere (Ar or N2); 20°C; not isolated; 1(H)-NMR, IR, MS identification;
参考文献
Riviere-Baudet, M.; Riviere, P.; Khallaayoun, A.; Satge, J.; Rauzy, K.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 77 - 94
反应条件
in benzene
inert atmosphere (Ar or N2); 40°C, 24 h; fractional distn.;
参考文献
Riviere-Baudet, M.; Riviere, P.; Khallaayoun, A.; Satge, J.; Rauzy, K.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 77 - 94
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0°C; 0.0833333 h;
参考文献
Demmin, Timothy R.; Rogic, Milorad M.
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 1153 - 1156
反应条件
potassium peroxomonosulphate in 1,4-dioxane; water
T=10°C; phosphate buffer pH 7;
参考文献
Ando, Wataru; Miyazaki, Hajime; Akasaka, Takeshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 9 p. 518 - 519
