6,7-二甲氧基-3,4-二氢异喹啉合成路线 （共 75 条）
反应条件
tert.-butylhydroperoxide; tris(triphenylphosphine)ruthenium(II) chloride; palladium in decane Molecular sieve;
参考文献
Yu, Qian-Sheng; Luo, Weiming; Deschamps, Jeffery; Holloway, Harold W.; Kopajtic, Theresa; Katz, Jonathan L.; Brossi, Arnold; Greig, Nigel H.
ACS Medicinal Chemistry Letters, 2010 , vol. 1, # 3 p. 105 - 109
反应条件
trichlorophosphate in toluene
参考文献
Hillard, Russel L.; Parnell, Carol A.; Vollhardt, K. Peter C.
Tetrahedron, 1983 , vol. 39, # 6 p. 905 - 912
反应条件
oxygen; Ru2(O2CMe)4Cl in toluene T=50°C; P=760.051 Torr; 12 h;
参考文献
Synlett, , # 11 p. 1675 - 1678
反应条件
acetic acid; trifluoroacetic acid 5 h; Reflux;
参考文献
AUSPEX PHARMACEUTICAL ,INC.; GANT, Thomas, G.; SHAHBAZ, Manoucherhr
Patent: WO2010/44981 A2, 2010 ;
Location in patent: Page/Page column 28 ;
反应条件
1: 14 h; Reflux; 2: With phosphorus pentachloride in dichloromethane T=20°C; 2 h;
参考文献
Imbri, Dennis; Tauber, Johannes; Opatz, Till
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15080 - 15083
反应条件
air; 3-methyl-5-ethyllumiflavinium perchlorate in acetonitrile T=37°C; 552 h; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 53, # 14 p. 5027 - 5046
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene Decomposition; 4 h; Heating;
参考文献
Organic Letters, , vol. 2, # 3 p. 307 - 310
反应条件
1: 100 percent / methanol / 12 h / Ambient temperature 2: 89 percent / POCl3 / toluene View Scheme
参考文献
Tetrahedron, , vol. 39, # 6 p. 905 - 912
反应条件
sodium carbonate in water Inert atmosphere;
参考文献
Lalonde, Mathieu P.; McGowan, Meredeth A.; Rajapaksa, Naomi S.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2013 , vol. 135, # 5 p. 1891 - 1894
反应条件
nickel sulphate; sodium hydroxide; dipotassium peroxodisulfate in dichloromethane; water 1 h; Ambient temperature;
参考文献
Chemistry Letters, , # 5 p. 823 - 826
