乙基2-{[(4-甲基苯基)磺酰基]氧基}丙酸酯合成路线 (共 6 条)
反应条件
potassium fluoride; diethylene glycol
参考文献
Bergmann; Shahak
Chemistry and Industry (London, United Kingdom), 1958 , p. 157
参考文献
Hoffmann-La Roche Inc.
Patent: US4435207 A1, 1984 ;
反应条件
sodium in ammonia T=-78°C; 1 h;
参考文献
van Doorn, J. A.; Meijboom, N.
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 42, p. 211 - 222
反应条件
potassium carbonate in dichloromethane; acetonitrile
参考文献
Hoechst Aktiengesellschaft
Patent: US4531969 A1, 1985 ;
反应条件
borane-THF in tetrahydrofuran
1.) RT, 5 d, 2.) 40 to 50 deg C, 1 d; Yield given;
参考文献
Mori, Kenji; Senda, Shuji
Tetrahedron, 1985 , vol. 41, # 3 p. 541 - 546
反应条件
potassium carbonate in toluene; acetonitrile
参考文献
Hoechst Aktiengesellschaft
Patent: US4531969 A1, 1985 ;