5-甲基-2,3-二氢-1H-茚-1-醇合成路线 (共 4 条)
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Friedrich, Edwin C.; Tam, Teresa M.
Journal of Organic Chemistry, 1982 , vol. 47, # 2 p. 315 - 319
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Friedrich, Edwin C.; Tam, Teresa M.
Journal of Organic Chemistry, 1982 , vol. 47, # 2 p. 315 - 319
反应条件
1: 1,3,5-trinitrobenzene, sym-collidine / diethyl ether / 1.) room temp., 1.5 h, 2.) 50 deg C, 3 h 2: LiAlH4 / diethyl ether / 0.25 h / 0 °C View Scheme
参考文献
Friedrich, Edwin C.; Tam, Teresa M.
Journal of Organic Chemistry, 1982 , vol. 47, # 2 p. 315 - 319
反应条件
water in acetone T=39.5°C; other temperature; ΔH(excit.), ΔS(excit.); Rate constantKineticsThermodynamic data;
参考文献
Friedrich, Edwin C.; Tam, Teresa M.
Journal of Organic Chemistry, 1982 , vol. 47, # 2 p. 315 - 319