3-(二甲氧基膦酰基)-2-甲基丙酸甲酯合成路线 (共 7 条)
反应条件
hydrogen; palladium on activated charcoal in methanol P=2280 Torr; 24 h; Yield given. Title compound not separated from byproducts;
参考文献
Davidson, Robert M.; Kenyon, George L.
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2698 - 2703
反应条件
hydrogen; platinum(IV) oxide in ethyl acetate P=2280 Torr; 3 h; other catalysts;
参考文献
Davidson, Robert M.; Kenyon, George L.
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2698 - 2703
反应条件
1: 77 percent / 56percent NaH / 1,2-dimethoxy-ethane / 3 h / Ambient temperature 2: H2 / Pd-C / methanol / 24 h / 2280 Torr View Scheme
参考文献
Davidson, Robert M.; Kenyon, George L.
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2698 - 2703
反应条件
1: 1) NaH / benzene 1) 5h / r.t. 2) 3h r.t. 2: H2 / Platinum oxide / ethyl acetate / 3 h / 2280 Torr / other catalysts View Scheme
参考文献
Davidson, Robert M.; Kenyon, George L.
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2698 - 2703
参考文献
Pudowik; Arbusow
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 1837,1839;engl.Ausg.S.2035,2037
参考文献
Kamai; Kuchtin
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2372;engl.Ausg.S.2431
参考文献
Pudowik; Arbusow
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 1837,1839;engl.Ausg.S.2035,2037