2,3-二羟基丙基苯甲酸酯合成路线 （共 29 条）
反应条件
hydrogenchloride in tetrahydrofuran; water T=45 - 50°C;
参考文献
Lupin Limited
Patent: US2011/257396 A1, 2011 ;
Location in patent: Page/Page column 11 ;
反应条件
4-methylmorpholine N-oxide in water; acetone T=100°C; 3 h;
参考文献
Cano, Rafael; Perez, Juana M.; Ramon, Diego J.
Applied Catalysis A: General, 2014 , vol. 470, p. 177 - 182
反应条件
water in acetone T=80°C; P=7500600 Torr; 40 h;
参考文献
Kotsuki, Hiyoshizo; Kataoka, Masanori; Nishizawa, Hitoshi
Tetrahedron Letters, 1993 , vol. 34, # 25 p. 4031 - 4034
反应条件
ammonium cerium(IV) nitrate; silica gel in dichloromethane T=25°C; detritylation; 0.75 h;
参考文献
Hwu, Jih Ru; Jain, Moti L.; Tsai, Fu-Yuan; Tsay, Shwu-Chen; Balakumar, Arumugham; Hakimelahi, Gholam H.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5077 - 5088
参考文献
Wang, Yinglei; Zhi, Huizhen; Luo, Jun
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 379, p. 46 - 52
反应条件
trans-oct-2-enal; 4 A molecular sieve; oxygen; bis(3-methyl-2,4-pentanedionato)nickel(II) in 1,2-dichloro-ethane T=100°C; P=6080 Torr; 8 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mukaiyama, Teruaki; Imagawa, Kiyomi; Yamada, Tohru; Takai, Toshihiro
Chemistry Letters, 1992 , # 2 p. 231 - 234
反应条件
trifluoroacetic acid in acetonitrile T=25°C; detritylation; rearrangement;
参考文献
Hwu, Jih Ru; Jain, Moti L.; Tsai, Fu-Yuan; Tsay, Shwu-Chen; Balakumar, Arumugham; Hakimelahi, Gholam H.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5077 - 5088
参考文献
Piantadosi et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 6613,6616
反应条件
1: pyridine 2: aqueous HCl View Scheme
参考文献
Zhou, Ding; Lagoja, Irene M.; Van Aerschot, Arthur; Herdewijn, Piet
Collection of Czechoslovak Chemical Communications, 2006 , vol. 71, # 1 p. 15 - 34
反应条件
oxygen; potassium carbonate T=30°C; 24 h;
参考文献
Yasukawa, Tomohiro; Miyamura, Hiroyuki; Kobayashi, Shu
Chemistry - An Asian Journal, 2011 , vol. 6, # 2 p. 621 - 627
