(NE)-N-[(2-甲基苯基)亚甲基]羟胺合成路线 (共 26 条)
反应条件
MS3 Angstroem; oxygen; sodium acetate; triphenylphosphine; palladium dichloride in N,N-dimethyl-formamide T=80°C; P=760 Torr; 14 h;
参考文献
Wang, Jia-Rui; Fu, Yao; Zhang, Bei-Bei; Cui, Xin; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8293 - 8297
反应条件
sodium carbonate; acetic acid in methanol; water 2 h; Heating;
参考文献
Goda, Hiroshi; Ihara, Hirotaka; Hirayama, Chuichi; Sato, Makoto
Tetrahedron Letters, 1994 , vol. 35, # 10 p. 1565 - 1568
反应条件
manganese(IV) oxide; 4 A molecular sieve in dichloromethane 22 h; Heating;
参考文献
Kanno, Hisashi; Taylor, Richard J. K.
Synlett, 2002 , # 8 p. 1287 - 1290
反应条件
potassium hydroxide; hydroxylamine hydrochloride in water; dimethyl sulfoxide 0.5 h;
参考文献
Li, Chunbao; Zhang, Hang; Cui, Yi; Zhang, Shuanming; Zhao, Zheyuan; Choi, Michael C. K.; Chan, Albert S. C.
Synthetic Communications, 2003 , vol. 33, # 4 p. 543 - 546
反应条件
potassium hydroxide; hydroxylamine hydrochloride in water; dimethyl sulfoxide 0.416667 h;
参考文献
Li, Chunbao; Zhang, Hang; Cui, Yi; Zhang, Shuanming; Zhao, Zheyuan; Choi, Michael C. K.; Chan, Albert S. C.
Synthetic Communications, 2003 , vol. 33, # 4 p. 543 - 546
反应条件
manganese(IV) oxide; 4 A molecular sieve in dichloromethane 22 h; Heating;
参考文献
Kanno, Hisashi; Taylor, Richard J. K.
Synlett, 2002 , # 8 p. 1287 - 1290
参考文献
Nakaya, Ryotaro; Yasuda, Shigeo; Yorimitsu, Hideki; Oshima, Koichiro
Chemistry - A European Journal, 2011 , vol. 17, # 31 p. 8559 - 8561
反应条件
bis(trifluoromethyl)thioketene in dichloromethane
参考文献
Raasch,M.S.
Journal of Organic Chemistry, 1970 , vol. 35, p. 3470 - 3483
反应条件
(i) NaH, 1,2-dimethoxy-ethane, (ii) /BRN= 471223/; Multistep reaction;
参考文献
Wadsworth,W.S.; Emmons,W.D.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2816 - 2820
参考文献
Blatt
Journal of the American Chemical Society, 1939 , vol. 61, p. 3494,3497