N-叔丁基-α-苯基硝酮合成路线 (共 68 条)
反应条件
[Rh(pentamethylcyclopentadienyl)(MeCN)3](SbF6)2; 2,2,2-trimethylacetic acid in 1,2-dichloro-ethane T=80°C; 15 h; Schlenk techniqueInert atmosphereSealed tube; Reagent/catalystSolvent;
参考文献
Qi, Zisong; Wang, Mei; Li, Xingwei
Organic Letters, 2013 , vol. 15, # 21 p. 5440 - 5443
反应条件
[Rh(pentamethylcyclopentadienyl)(MeCN)3](SbF6)2; H218O; 2,2,2-trimethylacetic acid in 1,2-dichloro-ethane T=80°C; 12 h; Schlenk techniqueInert atmosphereSealed tube;
参考文献
Qi, Zisong; Wang, Mei; Li, Xingwei
Organic Letters, 2013 , vol. 15, # 21 p. 5440 - 5443
反应条件
benzoyl chloride in 1,4-dioxane 8 h; Yield given;
参考文献
Heine, Harold W.; Zibuck, Regina; VandenHeuvel, William J. A.
Journal of the American Chemical Society, 1982 , vol. 104, # 13 p. 3691 - 3694
反应条件
1-chlorobenzotriazole in benzene 12 h; Ambient temperature; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1297 - 1306
反应条件
in benzene 12 h; Ambient temperature; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1297 - 1306
反应条件
in benzene 12 h; Ambient temperaturethermal and photochemical reactions; var. solvents; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1297 - 1306
反应条件
sodium azide; Titanium(IV) oxide in water Irradiationprolonged irradiation of the suspension;
参考文献
Maldotti, Andrea; Amadelli, Rossano; Carassiti, Vittorio
Canadian Journal of Chemistry, 1988 , vol. 66, p. 76 - 80
反应条件
dibenzene sulfonimide; 2,4,6-tris(4-methoxyphenyl)pyrylium tetrafluoroborate in dichloromethane Irradiation; Title compound not separated from byproducts;
参考文献
Eberson, Lennart; Persson, Ola
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 5 p. 893 - 898
反应条件
2,4,6-tris(4-methoxyphenyl)pyrylium tetrafluoroborate in dichloromethane Irradiation; Title compound not separated from byproducts;
参考文献
Eberson, Lennart; Persson, Ola
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 5 p. 893 - 898
反应条件
di-tert-butyl peroxide in benzene T=70°C; Irradiationthe formation of nitroxyl radicals; Mechanism;
参考文献
Yarkov, S. P.; Miller, V. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 10 p. 1972 - 1975
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 10 p. 2239 - 2242