3-[(2-羟基乙基)氨基]丙腈合成路线 （共 6 条）
反应条件
T=50°C; 12 h; Neat (no solvent);
参考文献
APPLIED RESEARCH SYSTEMS ARS HOLDING N.V.
Patent: WO2005/26159 A1, 2005 ;
Location in patent: Page/Page column 38 ;
反应条件
T=30°C; pH 9.7, pH 10.2 und pH 10.8; Rate constant;
参考文献
Ogata et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 5426
反应条件
1: formic acid 2: Raney nickel; ammonia; ethanol / 120 °C / 66195.7 Torr / Hydrogenation View Scheme
参考文献
Ishiguro; Matsumura
Yakugaku Zasshi, 1959 , vol. 79, p. 153,156
Chem.Abstr., 1959 , p. 13163
反应条件
1: formic acid 2: Raney nickel; ammonia; ethanol / 120 °C / 66195.7 Torr / Hydrogenation 3: dioxane; Raney nickel; hydrogen / 200 °C / 51485.6 Torr View Scheme
参考文献
Ishiguro; Matsumura
Yakugaku Zasshi, 1959 , vol. 79, p. 153,156
Chem.Abstr., 1959 , p. 13163
反应条件
ethanol; ammonia; nickel T=120°C; P=66195.7 Torr; Hydrogenation;
参考文献
Surrey; Hammer
Journal of the American Chemical Society, 1950 , vol. 72, p. 1814
反应条件
1: Raney nickel; ammonia; ethanol / 120 °C / 66195.7 Torr / Hydrogenation
2: 150 - 170 °C
View Scheme
参考文献
Surrey; Hammer
Journal of the American Chemical Society, 1950 , vol. 72, p. 1814
