1: 4-methyl-benzaldehyde With Br3COOEt; dibenzoyl peroxide in chlorobenzene T=110°C; 24 h; 2: cyclohexylamine With triethylamine in chlorobenzene T=20°C; 1 h;
1: With copper(l) iodide; lithium tert-butylate in N,N-dimethyl-formamide; acetonitrile T=20°C; 0.0833333 h; Inert atmosphere; 2: in N,N-dimethyl-formamide; acetonitrile T=20°C; 24 h; Inert atmosphereIrradiation;
参考文献
Do, Hien-Quang; Bachman, Shoshana; Bissember, Alex C.; Peters, Jonas C.; Fu, Gregory C.
Journal of the American Chemical Society, 2014 , vol. 136, # 5 p. 2162 - 2167