1-叔丁基-3-甲氧基苯合成路线 (共 24 条)
反应条件
oxygen; copper diacetate; silver carbonate in N,N-dimethyl-formamide T=140°C; P=760.051 Torr; 36 h;
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Synthesis (Germany), 2013 , vol. 45, # 17 art. no. SS-2013-Z0414-PSP, p. 2387 - 2390
反应条件
1: 3-t-butylphenol With sodium hydride in N,N-dimethyl-formamide T=20°C; 0.166667 h; Inert atmosphere; 2: methyl iodide in N,N-dimethyl-formamide T=20°C;
参考文献
Anderson, Eric C.; Biediger, Ronald J.; Chen, Jie; Dupre, Brian; Lory, Pedro; Market, Robert V.; Monk, Keith A.; Savage, Michael M.; Tennyson, Reginald; Young, Brandon M.
Patent: US2010/29753 A1, 2010 ;
Location in patent: Page/Page column 24-25 ;
US 20100029753 A1
反应条件
sodium hydroxide T=120°C; 0.5 h;
参考文献
Kitagawa, Toshikazu; Miyabo, Atsushi; Fujii, Hideki; Okazaki, Takao; Mori, Tetsuya; Matsudou, Masaki; Sugie, Takeshi; Takeuchi, Ken'ichi
Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 888 - 892
反应条件
1.54H2O*Cl2Ni; ICy*HBF4 in tetrahydrofuran T=-10°C; Kumada coupling reaction; 1.5 h; Inert atmosphere;
参考文献
Joshi-Pangu, Amruta; Wang, Chao-Yuan; Biscoe, Mark R.
Journal of the American Chemical Society, 2011 , vol. 133, # 22 p. 8478 - 8481
反应条件
1.54H2O*Cl2Ni; ICy*HBF4 in tetrahydrofuran T=-10°C; Kumada coupling reaction; 1.5 h; Inert atmosphere;
参考文献
Joshi-Pangu, Amruta; Wang, Chao-Yuan; Biscoe, Mark R.
Journal of the American Chemical Society, 2011 , vol. 133, # 22 p. 8478 - 8481
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=90°C; Inert atmosphere;
参考文献
Tietze, Lutz F.; Vock, Carsten A.; Krimmelbein, Ilga K.; Nacke, Linda
Synthesis, 2009 , # 12 art. no. T20108SS, p. 2040 - 2060
反应条件
pyridine; bis(acetylacetonate)nickel(II) in toluene
参考文献
Jeffery,E.A. et al.
Australian Journal of Chemistry, 1974 , vol. 27, p. 2569 - 2576
反应条件
aluminium trichloride in neat (no solvent) T=80°C; time dependence of isomerization; Product distribution;
参考文献
Olah, George A.; Olah, Judith A.; Ohyama, Toshiyuki
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5284 - 5290
反应条件
aluminium trichloride in nitromethane T=25°C; time dependence of isomerization; Product distribution;
参考文献
Olah, George A.; Olah, Judith A.; Ohyama, Toshiyuki
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5284 - 5290
反应条件
aluminium trichloride in nitromethane T=25°C; 0.0833333 h; Product distribution;
参考文献
Olah, George A.; Olah, Judith A.; Ohyama, Toshiyuki
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5284 - 5290