4-苄氧基-3-甲氧基苯甲醇合成路线 （共 22 条）
反应条件
C77H60Cl2N4O4PRu2; 4-methylmorpholine N-oxide in dichloromethane 8 h; Reflux;
参考文献
Venkatachalam; Raja; Pandiarajan; Ramesh
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2008 , vol. 71, # 3 p. 884 - 891
反应条件
1: 93.5 percent / thionyl chloride / diethyl ether / 6 h 2: dimethylformamide / 168 h / Ambient temperature 3: 1.) cobaltous chloride hexahydrate, NaBH4, 2.) 3 N HCl / 1.) MeOH, 20 deg C, 1 h View Scheme
参考文献
Nasreen, Amber; Gundlach, Heidrun; Zenk, Meinhart H.
Phytochemistry, 1997 , vol. 46, # 1 p. 107 - 115
反应条件
1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.83 h / 0 °C 2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1.25 h / -78 °C / Inert atmosphere 2.2: 22 h / -78 - -50 °C / Inert atmosphere 3.1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr / Inert atmosphere View Scheme
参考文献
Allais, Florent; Pla, Thomas J. L.; Ducrot, Paul-Henri
Synthesis, 2011 , # 9 art. no. T14311SS, p. 1456 - 1464
反应条件
1: PBr3 / diethyl ether 2: (i) nBuLi, THF, (ii) /BRN= 2130929/, (iii) aq. NaIO4, MeOH 3: H2 / Pd-C / methanol View Scheme
参考文献
Chemische Berichte, , vol. 112, # 11 p. 3703 - 3714
反应条件
thionyl chloride in diethyl ether 6 h;
参考文献
Nasreen, Amber; Gundlach, Heidrun; Zenk, Meinhart H.
Phytochemistry, 1997 , vol. 46, # 1 p. 107 - 115
反应条件
1: SOCl2 / dioxane / 20 °C 2: acetonitrile / 20 °C View Scheme
参考文献
Waddell, Thomas G.; Rapoport, Henry
Phytochemistry (Elsevier), 1985 , vol. 24, # 3 p. 469 - 472
反应条件
1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.83 h / 0 °C 2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1.25 h / -78 °C / Inert atmosphere 2.2: 22 h / -78 - -50 °C / Inert atmosphere 3.1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr / Inert atmosphere 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -15 °C View Scheme
参考文献
Allais, Florent; Pla, Thomas J. L.; Ducrot, Paul-Henri
Synthesis, 2011 , # 9 art. no. T14311SS, p. 1456 - 1464
反应条件
1: PBr3 / diethyl ether 2: dimethylformamide 3: LiAlH4 / diethyl ether View Scheme
参考文献
Waddell, Thomas G.; Rapoport, Henry
Phytochemistry (Elsevier), 1985 , vol. 24, # 3 p. 469 - 472
反应条件
phosphorus tribromide in diethyl ether
参考文献
Matsumoto, Shogo; Asakawa, Tomohiro; Hamashima, Yoshitaka; Kan, Toshiyuki
Synlett, 2012 , vol. 23, # 7 p. 1082 - 1084
反应条件
pyridinium hydrobromide perbromide in methanol
2 h; Ambient temperature;
参考文献
Wunsch; Nerdinger
Archiv der Pharmazie, 1995 , vol. 328, # 4 p. 301 - 305
