3,3-二氯戊烷-2,4-二酮合成路线 (共 7 条)
反应条件
tetrachlorosilane; urea hydrogen peroxide addition compound in dichloromethane T=0°C; 1.5 h;
参考文献
El-Ahl, Abdel Aziz S.; Elbeheery, Akram H.; Amer, Fathy A.
Synthetic Communications, 2011 , vol. 41, # 10 p. 1508 - 1513
反应条件
1,5-diazabicyclo[5.4.0]undeca-5-ene in dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
in dichloromethane 1:1 molar mixture of educts per acidic hydrogen, 20-25°C, 1 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
chlorine T=55 - 60°C;
参考文献
Amriev; Velichko; Abdulkina
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 111 pt 1 p. 2318 - 2322
反应条件
nitryl chloride in dichloromethane T=40°C; 2 h; 1) variation of molar ratio of NO2Cl/educt; Product distribution;
参考文献
Prostenik, Mladen V.; Dumic, Miljenko; Bosnjak, Nada
Monatshefte fuer Chemie, 1980 , vol. 111, p. 771 - 774
反应条件
1-hexene; manganese triacetate; copper dichloride T=40°C; 0.0166667 h; influence of additives; Product distributionMechanism;
参考文献
Vinogradov, M. G.; Dolinko, V. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 10 p. 2036 - 2041
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 10 p. 2313 - 2318
反应条件
triethylamine in tetrahydrofuran T=50°C;
参考文献
Russian Journal of Organic Chemistry, , vol. 45, # 9 p. 1412 - 1413