4,4''-二氨基对三联苯合成路线 （共 8 条）
反应条件
palladium 10 on activated carbon; hydrazine in ethanol 6 h; Inert atmosphereReflux;
参考文献
Meng, Wenjing; Clegg, Jack K.; Nitschke, Jonathan R.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 8 p. 1881 - 1884
反应条件
1: fuming HNO3 / acetic acid 2: SnCl2, aq. HCl View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 4370 - 4374
反应条件
1: 76 percent / K2CO3 / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 18 h / Heating 2: 99 percent / H2 / Pd/C / tetrahydrofuran / 18 h View Scheme
参考文献
Synthetic Communications, , vol. 36, # 10 p. 1343 - 1346
反应条件
1: 76 percent / K2CO3 / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 18 h / Heating 2: 99 percent / H2 / Pd/C / tetrahydrofuran / 18 h View Scheme
参考文献
Synthetic Communications, , vol. 36, # 10 p. 1343 - 1346
反应条件
1: N-bromosuccinmide; sulfuric acid / 60 °C 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 48 h / Reflux; Inert atmosphere 3: palladium 10 on activated carbon; hydrazine / ethanol / 6 h / Inert atmosphere; Reflux View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 8 p. 1881 - 1884
反应条件
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 48 h / Reflux; Inert atmosphere 2: palladium 10 on activated carbon; hydrazine / ethanol / 6 h / Inert atmosphere; Reflux View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 8 p. 1881 - 1884
反应条件
calcium carbonate in N-methyl-acetamide; water
参考文献
Khromov-Borisov; Nikolai V.; Torf; Samuil F.; Cherepanova; Valentina P.; Danilov; Anatoly F.
Patent: US4137239 A1, 1979 ;
反应条件
hydrogenchloride
Diazotization.Einleiten von Wasserdampf;
参考文献
Price; Mueller
Journal of the American Chemical Society, 1944 , vol. 66, p. 634
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Vorlaender
Chemische Berichte, 1937 , vol. 70, p. 1202,1210
