2,3,4-三邻苄基-l-岩藻吡喃糖合成路线 (共 17 条)
反应条件
10Pd/Al2O3; ammonium formate in methanol T=20°C; 10 h; optical yield given as percent deregioselective reaction;
参考文献
Jalsa, Nigel Kevin
Tetrahedron Letters, 2011 , vol. 52, # 49 p. 6587 - 6590
反应条件
hydrogenchloride; acetic acid in water T=95 - 100°C; 2 h;
参考文献
Nishi, Yuki; Tanimoto, Toshiko
Bioscience, Biotechnology and Biochemistry, 2009 , vol. 73, # 3 p. 562 - 569
反应条件
boron trifluoride diethyl etherate in dichloromethane T=40°C;
参考文献
Hendel, Jenifer L.; Wang, Jo-Wen; Jackson, Trudy A.; Hardmeier, Karolyn; De Los Santos, Richelle; Auzanneau, France-Isabelle
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8321 - 8331
反应条件
sulfuric acid in acetic acid T=90°C; 0.333333 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kondo, Hirosato; Aoki, Shin; Ichikawa, Yoshitaka; Halcomb, Randall L.; Ritzen, Helena; Wong, Chi-Huey
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 864 - 877
反应条件
N-bromosuccinmide; water in acetone T=20°C; 3 h; optical yield given as percent de;
参考文献
Matwiejuk, Martin; Thiem, Joachim
European Journal of Organic Chemistry, 2011 , # 29 p. 5860 - 5878
反应条件
chloramine-T in acetonitrile T=20°C; 1 h; Title compound not separated from byproducts;
参考文献
Misra, Anup Kumar; Agnihotri, Geetanjali
Carbohydrate Research, 2004 , vol. 339, # 4 p. 885 - 890
反应条件
palladium dichloride in methanol T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Khatuntseva, Elena A.; Ustuzhanina, Nadezhda E.; Zatonskii, Georgij V.; Shashkov, Alexander S.; Usov, Anatoly I.; Nifant'ev, Nikolay E.
Journal of Carbohydrate Chemistry, 2000 , vol. 19, # 9 p. 1151 - 1173
反应条件
iodine; sodium hydrogencarbonate in tetrahydrofuran; water T=20°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Khatuntseva, Elena A.; Ustuzhanina, Nadezhda E.; Zatonskii, Georgij V.; Shashkov, Alexander S.; Usov, Anatoly I.; Nifant'ev, Nikolay E.
Journal of Carbohydrate Chemistry, 2000 , vol. 19, # 9 p. 1151 - 1173
反应条件
1: NaH / dimethylformamide / 1.) 60 deg C, 30 min, 2.) 40 - 50 deg C, overnight 2: 3 M sulfuric acid / acetic acid / 0.33 h / 90 °C View Scheme
参考文献
Kondo, Hirosato; Aoki, Shin; Ichikawa, Yoshitaka; Halcomb, Randall L.; Ritzen, Helena; Wong, Chi-Huey
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 864 - 877
反应条件
1: methanol / Heating 2: NaH / dimethylformamide / 1.) 60 deg C, 30 min, 2.) 40 - 50 deg C, overnight 3: 3 M sulfuric acid / acetic acid / 0.33 h / 90 °C View Scheme
参考文献
Kondo, Hirosato; Aoki, Shin; Ichikawa, Yoshitaka; Halcomb, Randall L.; Ritzen, Helena; Wong, Chi-Huey
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 864 - 877