(1-溴甲基-乙烯基)-苯合成路线 （共 50 条）
反应条件
pyrrolidine; pyrrolidin-1-yl-2,5-dione; N-bromosuccinmide in chloroform T=60°C; 3 h;
参考文献
Zhu, Mingzhao; Lin, Shuangzheng; Zhao, Gui-Ling; Sun, Junliang; Cordova, Armando
Tetrahedron Letters, 2010 , vol. 51, # 20 p. 2708 - 2712
参考文献
Wei, Ying; Liang, Fushun; Zhang, Xintong
Organic Letters, 2013 , vol. 15, # 20 p. 5186 - 5189
反应条件
1: NBS, benzoyl peroxide / CCl4 / 18 h / Heating 2: p-toluolsulphonic acid 3: NBS, benzoyl peroxide / CCl4 / 18 h / Heating 4: p-toluolsulphonic acid View Scheme
参考文献
Ravindranath, B.; Srinivas, P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 592 - 594
参考文献
Posner, Gary H.; Wang, Dasong; Gonzalez, Lluisa; Tao, Xueliang; Cumming, Jared N.; Klinedinst, Donna; Shapiro, Theresa A.
Tetrahedron Letters, 1996 , vol. 37, # 6 p. 815 - 818
反应条件
N-bromosuccinmide in chlorobenzene 0.25 h; Heating; Title compound not separated from byproducts;
参考文献
Raubo, Piotr; Kulagowski, Janusz J.; Chicchi, Gary G.
Synlett, 2006 , # 2 p. 271 - 274
反应条件
1: p-toluolsulphonic acid 2: NBS, benzoyl peroxide / CCl4 / 18 h / Heating 3: p-toluolsulphonic acid View Scheme
参考文献
Ravindranath, B.; Srinivas, P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 592 - 594
反应条件
para-toluenesulphonic acid silver salt in dichloromethane 1 h; Ambient temperature;
参考文献
Oki, Michinori; Shionoiri, Katsumi; Otake, Katsumasa; Ono, Masaru; Toyota, Shinji
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 2 p. 589 - 597
反应条件
1.1: magnesium / diethyl ether / 2 h / 0 °C / |Reflux 1.2: 0.5 h / 20 °C 1.3: 24 h / |Reflux 2.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C 2.2: 3 h / 0 °C View Scheme
参考文献
Garzan, Atefeh; Jaganathan, Arvind; Salehi Marzijarani, Nastaran; Yousefi, Roozbeh; Whitehead, Daniel C.; Jackson, James E.; Borhan, Babak
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9015 - 9021
反应条件
1.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C / |Inert atmosphere 1.2: 16 h / 0 - 20 °C / |Inert atmosphere 2.1: N-bromosuccinmide; toluene-4-sulfonic acid / tetrahydrofuran / 4 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Tripathi, Chandra Bhushan; Mukherjee, Santanu
Angewandte Chemie - International Edition, 2013 , vol. 52, # 32 p. 8450 - 8453
Angew. Chem., 2013 , vol. 125, # 32 p. 8608 - 8611,4
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane 18 h; Heating; Yield given. Yields of byproduct given;
参考文献
Ravindranath, B.; Srinivas, P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 592 - 594
