(1-溴甲基-乙烯基)-苯合成路线 (共 50 条)
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid
参考文献
Wyrick, Steven D.; Booth, Raymond G.; Myers, Andrew M.; Owens, Constance E.; Bucholtz, Ehren C.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 19 p. 3857 - 3864
反应条件
1: With triphenylphosphine in dichloromethane T=0°C; 0.166667 h; 2: With carbon tetrabromide in dichloromethane T=0°C; 3 h;
参考文献
Garzan, Atefeh; Jaganathan, Arvind; Salehi Marzijarani, Nastaran; Yousefi, Roozbeh; Whitehead, Daniel C.; Jackson, James E.; Borhan, Babak
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9015 - 9021
反应条件
N-bromosuccinmide; toluene-4-sulfonic acid in tetrahydrofuran T=100°C; 4 h; Inert atmosphere;
参考文献
Tripathi, Chandra Bhushan; Mukherjee, Santanu
Angewandte Chemie - International Edition, 2013 , vol. 52, # 32 p. 8450 - 8453
Angew. Chem., 2013 , vol. 125, # 32 p. 8608 - 8611,4
反应条件
1: With ammonium metavanadate; tetrabutylammomium bromide; toluene-4-sulfonic acid in water; acetonitrile T=20°C; 12 h; 2: With silica gel in hexane; ethyl acetate Column chromatography;
参考文献
Kikushima, Kotaro; Moriuchi, Toshiyuki; Hirao, Toshikazu
Chemistry - An Asian Journal, 2009 , vol. 4, # 8 p. 1213 - 1216
反应条件
magnesium bromide in diethyl ether T=20°C; 0.5 h;
参考文献
Kozyrkov, Yurii Yu.; Kulinkovich, Oleg G.
Synlett, 2002 , # 3 p. 443 - 446
反应条件
N-bromosuccinmide in chloroform
参考文献
Japan Science and Technology Agency; Wako Pure Chemical Industries, Ltd.; FUJI PHOTO FILM CO., LTD.; Kobayashi, Shu
Patent: EP1739104 A1, 2007 ;
反应条件
carbon monoxide in diethylene glycol heating in diglime at 140°C for 0.5 h under CO atm. ;;
参考文献
Nagashima, Hideo; Mukai, Katsunori; Itoh, Kenji
Organometallics, 1984 , vol. 3, p. 1314 - 1315
反应条件
boron trifluoride diethyl etherate in benzene 2 h; Heating;
参考文献
Bettadaiah; Srinivas
Synthetic Communications, 2003 , vol. 33, # 20 p. 3615 - 3620
反应条件
N-bromosuccinmide; n-Bu4NH2F3 in dichloromethane 1 h; Heating;
参考文献
Albanese, Domenico; Landini, Dario; Penso, Michele; Pratelli, Marco
Gazzetta Chimica Italiana, 1991 , vol. 121, # 12 p. 537 - 541
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane HeatingIrradiation;
参考文献
Vaccher; Berthelot; Flouquet; Debaert
Synthetic Communications, 1993 , vol. 23, # 5 p. 671 - 679