N-异丙基-1,3-丙二胺合成路线 （共 6 条）
反应条件
ammonia; nickel T=120°C; P=128714 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1218
反应条件
diethyl ether Hydrogenation.Hydrieren eines Gemisches des Reaktionsprodukts mit Ammoniak an Raney-Nickel bei 100grad/140at;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2016
反应条件
in ethyl acetate 54 h;
参考文献
Journal of the American Chemical Society, , vol. 129, # 24 p. 7627 - 7637
反应条件
(i) EtOH, (ii) LiAlH4; Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 15, p. 228 - 232
反应条件
1: 56 percent / p-toluenesulfonic acid monohydrate / 5 h / 210 °C
2: 97 percent / diisobutylaluminum hydride / hexane / 1.) 25 deg C, 1 d, 2.) reflux, 30 min
View Scheme
参考文献
Yamamoto,H.; Maruoka,K.
Journal of the American Chemical Society, 1981 , vol. 103, p. 4186
参考文献
Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1208,1210
Full Text Show Details
Pearson; Jones; Cope
Journal of the American Chemical Society, 1946 , vol. 68, p. 1227
