O-(4-硝基苯基)羟胺合成路线 （共 24 条）
反应条件
1: With hydrogenchloride; water T=25 - 32°C; 1 h; 2: With sodium hydroxide in water T=33°C; Product distribution / selectivity;
参考文献
CAMBREX KARLSKOGA AB; HANSSON, Lars, O.; BERGH, Anders; ELKUND, Lars
Patent: WO2010/116140 A1, 2010 ;
Location in patent: Page/Page column 47 ;
反应条件
antimony(V) pentachloride in benzene T=180°C; 5 h;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
1: 92 percent / K2CO3 / dimethylformamide / 50 °C 2: 72 percent / hydazine monohydrate / CH2Cl2 / Heating View Scheme
参考文献
Sheradsky,T. et al.
Tetrahedron, 1972 , vol. 28, p. 3833 - 3843
反应条件
1: With potassium tert-butylate in methanol 2: With O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine in N,N-dimethyl-formamide T=0°C; 0.5 h;
参考文献
Salahuddin, Syed; Renaudet, Olivier; Raymond, Jean-Louis
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 10 p. 1471 - 1475
反应条件
4-nitro-phenol; antimony(V) pentachloride in benzene T=180°C; 5 h;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
1: SOCl2 / 3 h / Heating 2: 73 percent Chromat. / p-nitrophenol, SbCl5 / benzene / 5 h / 180 °C View Scheme
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
1: 25.4 percent / 5 h / 180 °C 2: 73 percent / SbCl5 / benzene / 5 h / 180 °C View Scheme
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
T=180°C; 72 h; Further byproducts given;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
1: 65 percent / t-BuOK / dimethylformamide / 0.5 h / 0 °C 2: 70 percent / HClO4 / H2O / 2 h / 0 °C View Scheme
参考文献
SANOFI; BAILLY, Frederic; BON, Xavier; VAYRON, Philippe
Patent: US2013/165674 A1, 2013 ;
反应条件
T=180°C; 72 h; Further byproducts given;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
