2-[(2-甲基丙烷-2-基)氧基]乙基苯合成路线 (共 5 条)
反应条件
sulfuric acid; magnesium sulfate in cyclohexane T=25°C; 18 h;
参考文献
Wright, Stephen W.; Hageman, David L.; Wright, Ann S.; McClure, Lester D.
Tetrahedron Letters, 1997 , vol. 38, # 42 p. 7345 - 7348
反应条件
boron trifluoride diethyl etherate in cyclohexane 19 h; Ambient temperature;
参考文献
Armstrong, Alan; Brackenridge, Ian; Jackson, Richard F.W.; Kirk, Joanna M.
Tetrahedron Letters, 1988 , vol. 29, # 20 p. 2483 - 2486
反应条件
SaSA in hexane 1 h; Reflux;
参考文献
Shirini; Zolfigol; AbediniM.
Journal of the Iranian Chemical Society, 2010 , vol. 7, # 3 p. 603 - 607
反应条件
Pd-PEPPSI-IPr; potassium carbonate in water; toluene T=120°C; Suzuki-Miyaura coupling; 24 h; Inert atmosphere;
参考文献
Colombel, Virginie; Rombouts, Frederik; Oehlrich, Daniel; Molander, Gary A.
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2966 - 2970
反应条件
potassium tert-butylate; sec.-butyllithium; lithium bromide 1.) cyclohexane, THF, -78 deg C, 2 h, then -10 deg C, 30 min, 2.) -78 deg C, THF; Yield given. Multistep reaction;
参考文献
Corey, E. J.; Eckrich, Thomas M.
Tetrahedron Letters, 1983 , vol. 24, # 31 p. 3165 - 3168