3-(2-甲氧基-苯基)-丙醛合成路线 （共 19 条）
反应条件
oxygen; palladium diacetate; copper(l) chloride in dimethyl sulfoxide T=50°C; P=760.051 Torr; 20 h; regioselective reaction;
参考文献
Chen, Mao; Wang, Jie; Chai, Ziyi; You, Cai; Lei, Aiwen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 341 - 346
反应条件
dimethyl sulfoxide; triethylamine in dichloromethane; water
参考文献
Sankyo Company, Limited
Patent: US5556864 A1, 1996 ;
US 5556864 A
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate T=80°C; 30 h;
参考文献
Gangjee, Aleem; Qiu, Yibin; Kisliuk, Roy L.
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 6 p. 941 - 946
反应条件
Rh(acetylacetonate)(CO)2; C75H54N4O8P2; hydrogen in dichloromethane T=20°C; P=15001.5 Torr; 72 h; Autoclave; Reagent/catalyst; regioselective reaction;
参考文献
Dydio, Pawel; Detz, Remko J.; De Bruin, Bas; Reek, Joost N. H.
Journal of the American Chemical Society, 2014 , vol. 136, # 23 p. 8418 - 8429
反应条件
1: methanol 2: DIBAL / tetrahydrofuran / -40 °C 3: MnO2 / acetone; CH2Cl2 4: H2 / Pd/C / methanol 5: Swern oxidating reagent View Scheme
参考文献
Kwon, Byoung-Mog; Lee, Seung-Ho; Cho, Young-Kwon; Bok, Song-Hae; So, Seung-Ho; Youn, Mi-Ran; Chang, Soo-Ik
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 19 p. 2473 - 2476
反应条件
1: MnO2 / acetone; CH2Cl2 2: H2 / Pd/C / methanol 3: Swern oxidating reagent View Scheme
参考文献
Kwon, Byoung-Mog; Lee, Seung-Ho; Cho, Young-Kwon; Bok, Song-Hae; So, Seung-Ho; Youn, Mi-Ran; Chang, Soo-Ik
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 19 p. 2473 - 2476
反应条件
1: H2 / Pd/C / methanol 2: Swern oxidating reagent View Scheme
参考文献
Kwon, Byoung-Mog; Lee, Seung-Ho; Cho, Young-Kwon; Bok, Song-Hae; So, Seung-Ho; Youn, Mi-Ran; Chang, Soo-Ik
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 19 p. 2473 - 2476
反应条件
1: DIBAL / tetrahydrofuran / -40 °C 2: MnO2 / acetone; CH2Cl2 3: H2 / Pd/C / methanol 4: Swern oxidating reagent View Scheme
参考文献
Kwon, Byoung-Mog; Lee, Seung-Ho; Cho, Young-Kwon; Bok, Song-Hae; So, Seung-Ho; Youn, Mi-Ran; Chang, Soo-Ik
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 19 p. 2473 - 2476
反应条件
pyridine; lead(IV) acetate
参考文献
Kwon, Byoung-Mog; Lee, Seung-Ho; Cho, Young-Kwon; Bok, Song-Hae; So, Seung-Ho; Youn, Mi-Ran; Chang, Soo-Ik
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 19 p. 2473 - 2476
反应条件
1: pyridinium chlorochromate / dichloromethane 2: sodium hydride / tetrahydrofuran 3: hydrogen; palladium on activated charcoal / ethyl acetate 4: lithium aluminium tetrahydride / tetrahydrofuran 5: pyridinium chlorochromate / dichloromethane View Scheme
参考文献
Mimori, Seisuke; Okuma, Yasunobu; Kaneko, Masayuki; Kawada, Koichi; Nomura, Yasuyuki; Murakami, Yasuoki; Hamana, Hiroshi
Chemistry Letters, 2013 , vol. 42, # 9 p. 1051 - 1052
