三[2-(二甲氨基)乙基]胺合成路线 （共 6 条）
反应条件
formic acid in water T=120°C; 6 h;
参考文献
He, Guping; Zhang, Ganwei; Hu, Jiwen; Sun, Jianping; Hu, Shenyu; Li, Yinhui; Liu, Feng; Xiao, Dingshu; Zou, Hailiang; Liu, Guojun
Journal of Fluorine Chemistry, 2011 , vol. 132, # 9 p. 562 - 572
反应条件
1: With acetic acid in water; acetonitrile 1 h; 2: With sodium tetrahydroborate in water; acetonitrile T=0°C; 48 h;
参考文献
Fu, Shao; Liu, Yongdong; Ding, Yong; Du, Xiaoqiang; Song, Fangyuan; Xiang, Rui; Ma, Baochun
Chemical Communications, 2014 , vol. 50, # 17 p. 2167 - 2169
反应条件
in water T=100°C; Cooling with iceInert atmosphere;
参考文献
The University of Akron; Pugh, Coleen R.; Singh, Anirudha
Patent: US8524942 B2, 2013 ;
Location in patent: Page/Page column 21 ;
反应条件
hydrogenchloride; formaldehyd in water T=120°C; 6 h;
参考文献
Hong, Sung Woo; Ahn, Cheol-Hee; Huh, June; Jo, Won Ho
Macromolecules, 2006 , vol. 39, # 22 p. 7694 - 7700
参考文献
Justus Liebigs Annalen der Chemie, , vol. 575, p. 18,29
反应条件
n-butyllithium in pentane
a) 0 deg C, 1 h, b) RT, 1 h;
参考文献
Luitjes; Schakel; Klumpp
Synthetic Communications, 1994 , vol. 24, # 16 p. 2257 - 2261
