反应条件
1: 77 percent / PhCOCl / Heating 2: 70 percent / aq. NaOH, 30percent aq. H2O2 / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 1.) from -5 to -7 deg C, 2 min, 2.) 0 deg C 3: 1,1,2-trichloro-1,2,2-trifluoro-ethane / 20 °C / var. temp.; ΔH(excit.), ΔS(excit.) View Scheme
参考文献
Chengxue, Zhao; Renmo, Zhou; Heqi, Pan; Xiangshan, Jin; Yangling, Qu; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2009 - 2013
