(4-氯苯甲酰基)膦酸二甲酯合成路线 （共 5 条）
参考文献
Griffiths, D. Vaughan; Griffiths, Penelope A.; Whitehead, Belinda J.; Tebby, John C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 4 p. 479 - 484
反应条件
diethylamine in diethyl ether T=0°C; 1 h;
参考文献
Nguyen; Niesor; Bentzen
Journal of Medicinal Chemistry, 1987 , vol. 30, # 8 p. 1426 - 1433
反应条件
sodium hexamethyldisilazane 1) DMSO, toluene, 10-15 deg C, 5 min, 2) DMSO, 10-15 deg C, 15 min, 2 h 45 min, RT; Yield given. Multistep reaction;
参考文献
Hammerschmidt, Friedrich; Zbiral, Erich
Monatshefte fuer Chemie, 1980 , vol. 111, p. 1015 - 1024
参考文献
Griffiths, D. V.; Jamali, H. A. R.; Tebby, J. C.
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 25, p. 173 - 176
反应条件
1: With triethylaluminum in n-heptane; toluene
T=0°C; 0.166667 h; Inert atmosphere;
2: With water in n-heptane; toluene
Inert atmosphere;
参考文献
Seven, Ozlem; Polat-Cakir, Sidika; Hossain, Md. Shakhawoat; Emrullahoglu, Mustafa; Demir, Ayhan S.
Tetrahedron, 2011 , vol. 67, # 19 p. 3464 - 3469
