1-(4-溴苯基)-2-羟基乙基-1-酮合成路线 (共 22 条)
反应条件
1: With β-cyclodextrin in water; acetone T=20 - 60°C; 2: With N-bromosuccinmide in water; acetone T=20°C; 24 h;
参考文献
Arjun Reddy; Bhanumathi; Rama Rao
Tetrahedron Letters, 2002 , vol. 43, # 17 p. 3237 - 3238
反应条件
water T=125°C; 0.416667 h; microwave irradiation;
参考文献
Utsukihara, Takamitsu; Nakamura, Hiroaki; Watanabe, Masashige; Akira Horiuchi
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9359 - 9364
反应条件
3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=60°C; 24 h; Inert atmosphere;
参考文献
Kuhl, Nadine; Glorius, Frank
Chemical Communications, 2011 , vol. 47, # 1 p. 573 - 575
反应条件
Novozyme 435TM in ethanol T=20°C; 1.5 h;
参考文献
Paizs, Csaba; Tosa, Monica; Majdik, Cornelia; Bodai, Viktoria; Novak, Lajos; Irimie, Florin-Dan; Poppe, Laszlo
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 21 p. 2400 - 2402
反应条件
Oxonereg;; 3,3'-diiodo-2,2',6,6'-tetramethoxy-4,4'-biphenyldicarboxylic acid in nitromethane T=30 - 35°C; 13 h;
参考文献
Seth, Saona; Jhulki, Samik; Moorthy, Jarugu Narasimha
European Journal of Organic Chemistry, 2013 , # 12 p. 2445 - 2452
反应条件
water; dimethyl sulfoxide in acetonitrile T=20°C;
参考文献
Huang; Hou; Wang; Chen
Organic Preparations and Procedures International, 2006 , vol. 38, # 5 p. 473 - 476
反应条件
Oxonereg;; iodobenzene; trifluoroacetic anhydride in water; acetonitrile T=90°C; 15 h;
参考文献
Chen, Chengqun; Feng, Xinghua; Zhang, Guozhen; Zhao, Qin; Huang, Guosheng
Synthesis, 2008 , # 20 p. 3205 - 3208
反应条件
water T=125°C; 0.416667 h;
参考文献
Utsukihara, Takamitsu; Nakamura, Hiroaki; Watanabe, Masashige; Akira Horiuchi
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9359 - 9364
反应条件
sodium hydrogencarbonate in methanol; water 1.5 h; Heating;
参考文献
Waszkuc, Wieslaw; Janecki, Tomasz; Bodalski, Ryszard
Synthesis, 1984 , # 12 p. 1025 - 1027
反应条件
in acetone T=25°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 35, # 47 p. 8751 - 8754