羟基-(4-甲氧基苯基)甲烷磺酸钠盐合成路线 (共 10 条)
反应条件
sodium hydrogensulfite in ethanol; water 20.5 h; Inert atmosphere;
参考文献
Barniol-Xicota, Marta; Turcu, Andreea L.; Codony, Sandra; Escolano, Carmen; Vazquez, Santiago
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2548 - 2550
反应条件
Na2S2O5 in water T=25°C; pH=7; Rate constant;
参考文献
Basu, Sukumar; Schuster, Peter; Wolschann, Peter
Monatshefte fuer Chemie, 1981 , vol. 112, p. 421 - 428
反应条件
sodium tetrahydroborate; montmorillonite K-10 in acetonitrile T=20°C; 0.216667 h;
参考文献
Khodaei, Mohammad M.; Khosropour, Ahmad R.; Abbasi, Jamshide
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 1 p. 93 - 97
反应条件
piperazine in ethylene glycol Knoevenagel condensation; 0.075 h; microwave irradiation;
参考文献
Khosropour, Ahmad Reza; Khodaei, Mohammad Mehdi; Moghanian, Hassan
Journal of Chemical Research, 2005 , # 6 p. 364 - 365
反应条件
1: sodium 1-hydroxy-1-(4-methoxyphenyl)methanesulfonate With triethylamine in 1,2-dichloro-ethane T=20°C; 0.25 h; Inert atmosphere; 2: diethylamine in 1,2-dichloro-ethane T=20°C; 0.75 h; Inert atmosphere; 3: With sodium tris(acetoxy)borohydride in 1,2-dichloro-ethane T=20°C; 16.5 h; Inert atmosphere;
参考文献
Pandit, Chennagiri R.; Mani, Neelakandha S.
Synthesis, 2009 , # 23 art. no. M03009SS, p. 4032 - 4036
反应条件
in N,N-dimethyl-formamide T=130°C; 6 h;
参考文献
Qi, Yunkun; Ma, Ruixin; Li, Xin; Hu, Yue; Ma, Siti; Cong, Chao; Ma, Xiaodong; Cui, Wenping; Ma, Shutao
Letters in Drug Design and Discovery, 2011 , vol. 8, # 10 p. 966 - 971
反应条件
sodium cyanoborohydride in methanol
T=20°C; 20 h;
参考文献
Barniol-Xicota, Marta; Turcu, Andreea L.; Codony, Sandra; Escolano, Carmen; Vazquez, Santiago
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2548 - 2550
反应条件
1.) water, 100 deg C, 2 h; 2.) water, 30 deg C, 5 h; Multistep reaction;
参考文献
Astik, R. R.; Thaker, K. A.
Journal of the Indian Chemical Society, 1981 , vol. 58, p. 1013 - 1014
反应条件
sodium cyanoborohydride in methanol
T=20°C; 20 h;
参考文献
Barniol-Xicota, Marta; Turcu, Andreea L.; Codony, Sandra; Escolano, Carmen; Vazquez, Santiago
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2548 - 2550
反应条件
trichlorophosphate in acetonitrile
0.166667 h; Heating;
参考文献
Khosropour, Ahmad R.; Khodaei, Mohammad M.; Hoseini Jomor, Seyed J.
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 3 p. 683 - 686