(S)-(-)-3-羟基-3-苯基丙酸乙酯合成路线 (共 48 条)
反应条件
in ethanol T=0°C; transesterification; 20 h; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 65, # 6 p. 1702 - 1706
反应条件
1: immobilised Candida parapsilosis ATCC 7330 whole cells / H2O; ethanol / 6 h / 25 °C 2: 57 percent / immobilised Candida parapsilosis ATCC 7330 whole cells / H2O; ethanol / 6 h / 25 °C View Scheme
参考文献
Tetrahedron, , vol. 62, # 21 p. 5133 - 5140
反应条件
1: 60 percent / 6N HCl 2: 81 percent / K2CO3 / acetone / 24 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 13, # 18 p. 2039 - 2051
反应条件
1: DMSO/oxalyl chloride / CH2Cl2 / 2 h / -60 °C 2: piperidinium acetate / benzene / 2 h / Heating View Scheme
参考文献
Synthesis, , p. 305 - 311
反应条件
Candida rugose type VII lipase in octane T=20°C; 15 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
Candida rugose type VII lipase in octane T=20°C; 15 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
Candida rugose type VII lipase in octane T=20°C; 15 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
Candida rugose type VII lipase in octane T=20°C; 15 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
1: sodium t-butanolate; C28H27N2O7Rh / toluene / 0.5 h / 80 °C / |Inert atmosphere 2: sodium peroxoborate tetrahydrate; water / tetrahydrofuran / 0.3 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 69, # 17 p. 3551 - 3560
反应条件
1: sodium t-butanolate; C22H31N2O7Rh / toluene / 0.5 h / 80 °C / |Inert atmosphere 2: sodium peroxoborate tetrahydrate; water / tetrahydrofuran / 0.3 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 69, # 17 p. 3551 - 3560