2-(2-甲氧基苯基)-乙酰胺合成路线 (共 6 条)
反应条件
1: SOCl2 2: aq. NH3 View Scheme
参考文献
Ganser, Christopher; Lauermann, Eva; Maderer, Annett; Stauder, Torsten; Kramb, Jan-Peter; Plutizki, Stanislav; Kindler, Thomas; Moehler, Markus; Dannhardt, Gerd
Journal of Medicinal Chemistry, 2012 , vol. 55, # 22 p. 9531 - 9540
参考文献
Ganser, Christopher; Lauermann, Eva; Maderer, Annett; Stauder, Torsten; Kramb, Jan-Peter; Plutizki, Stanislav; Kindler, Thomas; Moehler, Markus; Dannhardt, Gerd
Journal of Medicinal Chemistry, 2012 , vol. 55, # 22 p. 9531 - 9540
参考文献
Kariyone; Imai
Yakugaku Zasshi, 1935 , vol. 55, p. 679,681; dtsch. Ref. S. 109
Chem. Zentralbl., 1935 , vol. 106, # II p. 3657
反应条件
1,4-dioxane; ammonium hydroxide; silver nitrate
参考文献
Seth; Deshapande
Journal of the Indian Chemical Society, 1950 , vol. 27, p. 429,431
反应条件
1: With boron tribromide in dichloromethane T=0 - 20°C; 1 h; 2: With water in dichloromethane T=0°C; 0.5 h;
参考文献
KOWA CO., LTD.
Patent: US2005/101636 A1, 2005 ;
Location in patent: Page/Page column 34 ;
反应条件
trichloromethyl chloroformate in various solvent(s) 0-5 deg C then heated to 60 deg C, 5 min;
参考文献
Bose, D. Subhas; Jayalakshmi, B.
Synthesis, 1999 , # 1 p. 64 - 65