N-Me-Val-OME盐酸盐合成路线 （共 14 条）
反应条件
hydrogenchloride; water in ethyl acetate T=20°C; 2 h;
参考文献
Chemistry - A European Journal, , vol. 17, # 3 p. 958 - 968
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol 4 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2437 - 2446
反应条件
1: diethyl ether 2: H2, 12 N HCl / 10percent Pd-C / methanol / 4 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2437 - 2446
反应条件
1: 91 percent / NaH / tetrahydrofuran / 24 h / Ambient temperature 2: 98 percent / diethyl ether / 0 °C 3: 92 percent / HCl / dioxane / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 16 p. 5542 - 5549
反应条件
thionyl chloride 16 h; Reflux;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 8, p. 2085 - 2090
反应条件
hydrogenchloride Ambient temperature;
参考文献
Synthesis, , # 1 p. 67 - 70
反应条件
1: 98 percent / diethyl ether / 0 °C 2: 92 percent / HCl / dioxane / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 16 p. 5542 - 5549
反应条件
hydrogenchloride 4 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1959 - 1968
反应条件
hydrogenchloride in ethyl acetate Substitution;
参考文献
Tetrahedron, , vol. 56, # 41 p. 8119 - 8131
反应条件
1: 98 percent 2: 87 percent / SOCl2 / 60 °C 3: 75 percent / Et3SiH, TFA / 0.5 h 4: 72 percent / HCl / Ambient temperature View Scheme
参考文献
Synthesis, , # 1 p. 67 - 70
