(2-甲基磺酰基苯基)-甲醇合成路线 （共 16 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=75°C;
参考文献
Huynh, Han Vinh; Yeo, Chun Hui; Chew, Ying Xia
Organometallics, 2010 , vol. 29, # 6 p. 1479 - 1486
反应条件
sodium methylate in methanol T=20°C; 72 h;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1460062 A1, 2004 ;
Location in patent: Page 68 ;
反应条件
borane-THF in tetrahydrofuran T=0 - 20°C; 4 h;
参考文献
Hiruta, Yuki; Watanabe, Takafumi; Nakamura, Etsuko; Iwasawa, Naoko; Sato, Hiroyasu; Hamada, Kensaku; Citterio, Daniel; Suzuki, Koji
RSC Advances, 2014 , vol. 4, # 19 p. 9791 - 9798
反应条件
1.1: NaOH / methanol 1.2: HCl / methanol 2.1: H2SO4 3.1: LiAlH4 / tetrahydrofuran 3.2: H2SO4 View Scheme
参考文献
Smith, Daniel J.; Yap, Glenn P.A.; Kelley, James A.; Schneider, Joel P.
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1513 - 1520
反应条件
NaY faujasite T=150°C; 26 h;
参考文献
Selva, Maurizio; Tundo, Pietro
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1464 - 1470
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Cadogan, J. I. G.; Husband, James B.; McNab Hamish
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 697 - 702
反应条件
roots of Conium maculatum in water T=20°C; 24 h; Enzymatic reaction;
参考文献
Salvano, Mario S.; Cantero, Juan J.; Vazquez, Ana M.; Formica, Stella M.; Aimar, Mario L.
Journal of Molecular Catalysis B: Enzymatic, 2011 , vol. 71, # 1-2 p. 16 - 21
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Ruwet,A.; Renson,M.
Bulletin des Societes Chimiques Belges, 1969 , vol. 78, p. 571 - 582
反应条件
1: (i) (diazotization), (ii) aq. Na2S2, (iii) aq. Na2S2O4,(iv) (methylation) 2: (i) SOCl2, (ii) /BRN= 1718733/ 3: LiAlH4 / tetrahydrofuran View Scheme
参考文献
Ruwet,A.; Renson,M.
Bulletin des Societes Chimiques Belges, 1969 , vol. 78, p. 571 - 582
反应条件
1: 95 percent 2: 89 percent / LiAlH4 View Scheme
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ferguson, George; Lough, Alan J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 875 - 880
