(Z)-3,7-二甲基-1,3,6-十八烷三烯合成路线 （共 26 条）
反应条件
hexacarbonyl molybdenum in toluene T=110°C; 72 h;
参考文献
Shimizu, Isao; Sakamoto, Toshiaki; Kawaragi, Saeko; Maruyama, Yooichiro; Yamamoto, Akio
Chemistry Letters, 1997 , # 2 p. 137 - 138
反应条件
sesquiterpene synthases Cop4 from Coprinus cinereus in terpene synthase buffer T=25°C; 18 h; Enzymatic reaction;
参考文献
Lopez-Gallego, Fernando; Agger, Sean A.; Abate-Pella, Daniel; Distefano, Mark D.; Schmidt-Dannert, Claudia
ChemBioChem, 2010 , vol. 11, # 8 p. 1093 - 1106
反应条件
chloro-trimethyl-silane; acetic anhydride in acetonitrile 24 h;
参考文献
Kumareswaran; Gupta, Anuradha; Vankar, Yashwant D.
Synthetic Communications, 1997 , vol. 27, # 2 p. 277 - 282
反应条件
germacrene A synthase from Nostoc sp. PCC7120 (NS1) in terpene synthase buffer T=25°C; 18 h; Enzymatic reaction;
参考文献
Lopez-Gallego, Fernando; Agger, Sean A.; Abate-Pella, Daniel; Distefano, Mark D.; Schmidt-Dannert, Claudia
ChemBioChem, 2010 , vol. 11, # 8 p. 1093 - 1106
反应条件
sesquiterpene synthases Cop6 from Coprinus cinereus in terpene synthase buffer T=25°C; 18 h; Enzymatic reaction;
参考文献
Lopez-Gallego, Fernando; Agger, Sean A.; Abate-Pella, Daniel; Distefano, Mark D.; Schmidt-Dannert, Claudia
ChemBioChem, 2010 , vol. 11, # 8 p. 1093 - 1106
反应条件
tetrakis(triphenylphosphine) palladium(0); 2-Propynylzinc bromide in tetrahydrofuran 3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Matsushita, Hajime; Negishi, Ei-ichi
Journal of Organic Chemistry, 1982 , vol. 47, # 21 p. 4161 - 4165
反应条件
anhydrous lithium acetate; copper diacetate; copper T=85 - 90°C;
参考文献
Uguen, D.
Tetrahedron Letters, 1984 , vol. 25, # 5 p. 541 - 542
反应条件
1: 86 percent 2: NaI / acetone / 1 h / 0 - 2 °C 3: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme
参考文献
Saplay, K. M.; Damodaran, N. P.; Dev, Sukh
Tetrahedron, 1983 , vol. 39, # 48 p. 2999 - 3004
反应条件
1: NaI / acetone / 1 h / 0 - 2 °C 2: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme
参考文献
Saplay, K. M.; Damodaran, N. P.; Dev, Sukh
Tetrahedron, 1983 , vol. 39, # 48 p. 2999 - 3004
反应条件
2: 86 percent 3: NaI / acetone / 1 h / 0 - 2 °C 4: triethylamine / hexane / 6 h / 25 °C / Irradiation View Scheme
参考文献
Saplay, K. M.; Damodaran, N. P.; Dev, Sukh
Tetrahedron, 1983 , vol. 39, # 48 p. 2999 - 3004
