4,4',4-三甲基-2,2':6',2-三联吡啶合成路线 (共 4 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=110°C; Substitution; Stille reaction; 16 h;
参考文献
Fallahpour
Synthesis, 2000 , # 12 p. 1665 - 1667
反应条件
1: 35 percent / PBr3 / 6 h / 175 °C 2: 55 percent / (Ph3P)4Pd / toluene / 16 h / 110 °C View Scheme
参考文献
Fallahpour
Synthesis, 2000 , # 12 p. 1665 - 1667
反应条件
1: 41 percent / CrO3, H2SO4 / 75 °C 2: 72 percent / H2SO4 / 72 h / Heating View Scheme
参考文献
Nazeeruddin; Pechy; Graetzel
Chemical Communications, 1997 , # 18 p. 1705 - 1706
反应条件
chromium(VI) oxide; sulfuric acid T=75°C;
参考文献
Nazeeruddin; Pechy; Graetzel
Chemical Communications, 1997 , # 18 p. 1705 - 1706