3,4-二氢-1-萘甲酸合成路线 （共 26 条）
反应条件
nBuNBF4; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=20°C; electrochemical reaction;
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
potassium acetate; [Pd(PPh3)2(OAc)2] in N,N-dimethyl-formamide T=25°C; 2 h;
参考文献
Cacchi, Sandro; Lupi, Alessandro
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3939 - 3942
反应条件
sodium in diethyl ether; ammonia 1 h;
参考文献
Bigge; Malone; Hays; Johnson; Novak; Lescosky; Retz; Ortwine; Probert Jr.; Coughenour; Boxer; Robichaud; Brahce; Shillis
Journal of Medicinal Chemistry, 1993 , vol. 36, # 14 p. 1977 - 1995
反应条件
sodium hydroxide; D,L-Cysteine in water T=20°C; Birch-type reduction; 3 h; UV-irradiation;
参考文献
Rabe
Chemische Berichte, 1898 , vol. 31, p. 1900
反应条件
potassium hydroxide in ethanol T=25°C; 13 h;
参考文献
Wuest, James D.
Tetrahedron, 1980 , vol. 36, # 91 p. 2291 - 2296
参考文献
Baeyer; Schoder
Justus Liebigs Annalen der Chemie, 1891 , vol. 266, p. 176
反应条件
sodium hydroxide in isopropyl alcohol T=20°C; Birch-type reduction; 6 h; UV-irradiation;
参考文献
Yoshimi, Yasuharu; Ishise, Akihiro; Oda, Hiromu; Moriguchi, Yousuke; Kanezaki, Hiroki; Nakaya, Yukari; Katsuno, Kayoko; Itou, Tatsuya; Inagaki, Sho; Morita, Toshio; Hatanaka, Minoru
Tetrahedron Letters, 2008 , vol. 49, # 21 p. 3400 - 3404
反应条件
sulfuric acid Erhitzen des Reaktionsprodukts mit wss. Natronlauge;
参考文献
Holmes; Mann
Journal of the American Chemical Society, 1947 , vol. 69, p. 2000,2002
Full Text Show Details
Fieser; Holmes
Journal of the American Chemical Society, 1936 , vol. 58, p. 2319,2321
Journal of the American Chemical Society, 1938 , vol. 60, p. 2548,2553
参考文献
Merck and Co., Inc.
Patent: US6166037 A1, 2000 ;
US 6166037 A
反应条件
1: triethylamine / diethyl ether / 0.83 h / Heating 2: 29 percent / diethyl ether / Heating 3: 73 percent / KOH / aq. ethanol / 13 h / 25 °C View Scheme
参考文献
Wuest, James D.
Tetrahedron, 1980 , vol. 36, # 91 p. 2291 - 2296
