5-氯-5H-二苯并磷杂环戊二烯合成路线 (共 8 条)
反应条件
phosphorus trichoride in tetrahydrofuran
参考文献
Johnson, Stephen E.; Knobler, Carolyn B.
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 115, p. 227 - 240
反应条件
1: With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 4 h; Inert atmosphere; 2: With phosphorus trichoride in tetrahydrofuran; pentane T=-198 - 20°C; Inert atmosphere;
参考文献
Fukazawa, Aiko; Kiguchi, Manabu; Tange, Satoshi; Ichihashi, Yasunori; Zhao, Qiang; Takahashi, Takuya; Konishi, Tatsuya; Murakoshi, Kei; Tsuji, Yuta; Staykov, Aleksandar; Yoshizawa, Kazunari; Yamaguchi, Shigehiro
Chemistry Letters, 2011 , vol. 40, # 2 p. 174 - 176
反应条件
(i) PCl3, CuBr, EtOAc, (ii) Al; Multistep reaction;
参考文献
Doak,G.O. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2382 - 2385
反应条件
(i) PCl5, (ii) P; Multistep reaction;
参考文献
Hellwinkel,D.; Krapp,W.
Chemische Berichte, 1978 , vol. 111, p. 13 - 41
参考文献
Chernyshev,E.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 800 - 804,806 - 809
参考文献
Chernyshev,E.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 800 - 804,806 - 809
参考文献
Chernyshev,E.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 800 - 804,806 - 809
参考文献
Doak,G.O. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2382 - 2385