七氟丙基1,2,2,2-四氟乙醚合成路线 (共 4 条)
反应条件
N,N-dimethyl-formamide T=130°C; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 21, p. 54
反应条件
1: With Cu2Cl2 in acetonitrile oligomerization; 2: With sodium carbonate in diethylene glycol dimethyl ether Elimination; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 12 p. 1715 - 1720
反应条件
sodium carbonate in diethylene glycol dimethyl ether T=115 - 130°C; other solvent; KineticsRate constantThermodynamic data;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 8 p. 1037 - 1039
Zhurnal Organicheskoi Khimii, , vol. 31, # 8 p. 1142 - 1144
反应条件
T=180°C; 40 h; thermal decomposition in an evacuated, sealed ampoule; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 16, p. 51 - 62